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Beilstein J. Org. Chem. 2017, 13, 2466–2472, doi:10.3762/bjoc.13.243
Graphical Abstract
Figure 1: 1H NMR analysis of QC-Br5 (Mn = 1,050, Ð = 1.11) after purification (in CDCl3).
Figure 2: Synthesis of PtBA homopolymers grafted from quercetin-based macroinitiator via seATRP under constan...
Figure 3: (a) First-order kinetic plot of seATRP with periodically applied different values of potential, bet...
Beilstein J. Org. Chem. 2015, 11, 392–402, doi:10.3762/bjoc.11.45
Figure 1: Preferential sites of cholesterol electrooxidation.
Scheme 1: Functionalization of the cholesterol side chain.
Scheme 2: Oxidation of cholestane-3β,5α,6β-triol triacetate (3) with the Gif system.
Scheme 3: Electrochemical oxidation of cholesteryl acetate (1a) with dioxygen and iron–picolinate complexes.
Scheme 4: Electrochemical chlorination of cholesterol catalyzed by FeCl3.
Scheme 5: Electrochemical chlorination of Δ5-steroids.
Scheme 6: Electrochemical bromination of Δ5-steroids in different solvents.
Scheme 7: Direct electrochemical acetoxylation of cholesterol at the allylic position.
Scheme 8: Direct anodic oxidation of cholesterol in dichloromethane.
Scheme 9: A plausible mechanism of the electrochemical oxidation of cholesterol in dichloromethane.
Scheme 10: The electrochemical formation of glycosides and glycoconjugates.
Scheme 11: Efficient electrochemical oxidation of cholesterol to cholesta-4,6-dien-3-one (24).
Beilstein J. Org. Chem. 2015, 11, 162–168, doi:10.3762/bjoc.11.16
Scheme 1: Synthesis of glycoconjugates from different cholesteryl donors.
Figure 1: Cyclic voltammograms registered in 0.2 M tetrabutylammonium tetrafluoroborate (TBABF4) in dichlorom...
Scheme 2: Electrochemical reaction of 3α,5α-cyclocholestan-6β-yl ethers 6a–h with 1,2:3,4-di-O-isopropylidene...
Scheme 3: Plausible mechanism of isomerization.